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Attempted hydroformylation of triacetyl-D-glucal Cameron, Christina Janet
Abstract
Triacetyl-D-glucal, an unsaturated sugar has been prepared and submitted to the hydroformylation reaction, which is the addition of carbon monoxide and hydrogen to an unsaturated compound at high pressure and temperature. A cobalt catalyst is generally used, in this case, cobalt acetate tetrahydrate. The mixture of products obtained was separated by column chromatography and distillation. The main products are probably triacetyl-D-deoxyglucose obtained by the addition of water to the starting material, 1,2-hydroglucal obtained by hydrogenation of the starting material, a small amount of the theoretical hydroformylation compound and varying amounts of the starting material.
Item Metadata
Title |
Attempted hydroformylation of triacetyl-D-glucal
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Creator | |
Publisher |
University of British Columbia
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Date Issued |
1955
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Description |
Triacetyl-D-glucal, an unsaturated sugar has been prepared and submitted to the hydroformylation reaction, which is the addition of carbon monoxide and hydrogen to an unsaturated compound at high pressure and temperature. A cobalt catalyst is generally used, in this case, cobalt acetate tetrahydrate.
The mixture of products obtained was separated by column chromatography and distillation. The main products are probably triacetyl-D-deoxyglucose obtained by the addition of water to the starting material, 1,2-hydroglucal obtained by hydrogenation of the starting material, a small amount of the theoretical hydroformylation compound and varying amounts of the starting material.
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Genre | |
Type | |
Language |
eng
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Date Available |
2012-02-10
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Provider |
Vancouver : University of British Columbia Library
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Rights |
For non-commercial purposes only, such as research, private study and education. Additional conditions apply, see Terms of Use https://open.library.ubc.ca/terms_of_use.
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DOI |
10.14288/1.0062389
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URI | |
Degree | |
Program | |
Affiliation | |
Degree Grantor |
University of British Columbia
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Campus | |
Scholarly Level |
Graduate
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Aggregated Source Repository |
DSpace
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Rights
For non-commercial purposes only, such as research, private study and education. Additional conditions apply, see Terms of Use https://open.library.ubc.ca/terms_of_use.